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      A zwitterionic monoalkylated derivative of [Pt₂(μ-S)₂(PPh₃)₄] from 1,3-propanesultone

      Ujam, Oguejiofo Theophilus; Henderson, William; Nicholson, Brian K.
      DOI
       10.1134/S0022476613030074
      Link
       link.springer.com
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      Citation
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      Ujam, O. T., Henderson, W. & Nicholson, B. K. (2013). A zwitterionic monoalkylated derivative of [Pt₂(μ-S)₂(PPh₃)₄] from 1,3-propanesultone. Journal of Structural Chemisty, 54(3), 523-527.
      Permanent Research Commons link: https://hdl.handle.net/10289/7893
      Abstract
      Reaction of dinuclear platinum(II) sulfido complex [Pt₂(μ-S)₂(PPh₃)₄] with 1,3-propanesultone gives the novel zwitterionic monoalkylated thiolate complex [Pt₂(μ-S){μ-S(CH₂)₃SO₃}•(PPh₃)₄], which was characterized by NMR spectroscopy, electrospray ionisation mass spectrometry, and a single crystal X-ray structure determination. Crystals are monoclinic, space group P2(1)/c with unit cell dimensions a = 16.8957(3) Å, b = 15.5031(3) Å, c = 28.0121(5) Å, β = 99.780(1)°, for Z = 4.
      Date
      2013
      Type
      Journal Article
      Publisher
      Springer
      Collections
      • Science and Engineering Papers [3011]
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